11.00 am – 12.00 pm Using and Maintenance of FTIR (Bruker Tensor 27) Mr.Pisipong Meunprasertdee 12.00 – 01.00 pm Launch 01.00 – 02.30 pm Workshop #1 Preparation of sample (KBr powder, KBr pellet) Workshop #2 Using FTIR (Bruker Tensor 27) 02.30 – 02.45 pm Coffee Break. Bruker “Tensor 27” spectrometer with “Hyperion 3000” FT-IR microscope Single element MCT detector 64.64 elements FPA detector 20x ATR (Ge crystal) objective 20x Ref-objective with macro-ATR-stage (600×600 µm FoV) GIR-objective 16x transmission and reflection objective “KnowItAll” software package for spectrum analysis “OPUS” software package Raman Microscope: LabRAM HR 800. Tool ID: J05 Bruker Corporation is an American manufacturer of scientific instruments for molecular and materials research, as well as for industrial and applied analysis The Bruker Tensor 27 FT-IR Spectrum System is a high performing yet compact spectrometer offering a multitude of automated features and easy operation. Includes: Computer.

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Contacts and Location

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Contact 1	Māra Grūbe
Enquire about this equipment
Organisational Unit	Institute of Microbiology and Biotechnology University of Latvia
Building	Rīga, Jelgavas 1
Room	529

Description

The VERTEX 70 provides the entry level of the Bruker VERTEX Series of high performance FT-IR spectrometers for demanding analytical and R&D application. The innovative instrument design results in PEAK flexibility and PEAK performance. The fully digital FT-IR spectrometer features DigiTectTM technology based on parallel running dual-channel delta sigma ADC´s with 24-bit dynamic range, the ACR and AAR Automatic Components and Accessories Recognition as well as the BRAIN Bruker Artificial Intelligence Network which guarantees PEAK signal-to-noise ratio and reliable user friendly instrument operation.

Specification

• Sealed and desiccated optics bench, optionally purgeable • RockSolidTM cube corner mirror based interferometer • Up to 5 exit and up to 2 input beam ports remotely selectable • Options for automated internal dual sources and dual detectors • Automatic sample compartment shutters optional • Easy beamsplitter exchange with permanent interferometer alignment • Wide range MIR & FIR beamsplitter covering 6000 to 10 cm-1 in one step • Near IR, visible/UV and far IR/THz spectral range extensions • Highest sensitivity due to parallel dual channel 24-bit dynamic range ADC´s • Unique Bruker BRAIN spectrometer technology • Rapid Scan, Slow Scan and Step Scan options for modulation and time resolved spectroscopy (TRS) • Complete and integrated OPUSTM operation and evaluation software • Availability of vacuum optics bench system VERTEX 70v

Services

The standard spectral resolution of better than 0.4 cm-1 is suitable for most measurements of solids, liquids and low temperature crystalline samples.

Funding Source

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• Stereolithography 3D printer – Ember Autodesk (DLP, 405 nm)

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• 3D printer SLS Sinterit Lisa

• 3D printer FDM A4V4 from 3ntr, temperature up to 450 °C, 3 filaments

• 3D filament extruder from 3devo, up to 450 °C, 700g/h

• Two size exclusion chromatography (Agilent 1200 series) equipped with both differential refractive index and UV detectors and an automatic sampler working in different solvents
• Size exclusion chromatography (Agilent 1100 series) equipped with a differential refractive index detector and an automatic sampler for determination of molecular weight parameters of water soluble polymers
• Size exclusion chromatography equipped with a PL LC 1120 injection pump, differential refractive index (ERMA 7517) and RALS/Visc (model T60B) integrated for triple detection measurements using the TriSec Win-03 software.
• Automatic Schott AVS 350/Ubbelohde capillary viscosimeter
• Automatic Knauer vapor phase osmometer/tonometer

under high/low pressure:

• Three autoclave reactors for high/low pressure polycondensation under inert atmosphere from Autoclave France (50-250ml)
• Two Agila PE20 hydraulic presses (high and low temperatures)
• Brabender single screw extruder (19 mm, 25D) which can be equipped with a ribbon die (50 x 0.5 mm) or a double-string die. A calendering machine UNIVEX and a conveyor belt can be connected to the extruder

at controlled temperature:

• Polyscience Cryostat (- 40 à + 100°C)
• Binder, Memmert, Heraeus thermostated (programmable), vacuum and ventilated ovens
• Heating baths and Julabo TD6 and Thermal H circulators (T<250°C)
• Eurostar Power Digi-Visc agitators
• IKA agitating and heating plates

under controlled atmosphere:

• Braun MB-130 gloves box with H₂O et O₂ (< 1 ppm) controllers and analyzers
• Brandsonic 2210 E-MTH ultrasonic bath

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• Brabender® blow film take-off unit
• Thermo Scientific Process 11 Twin-Screw Extruder (L/D=40, 11 mm), 20g/h to 2.5 kg/h
• Reactive extrusion (REX) equipments consisting in two Leistritz twin-screws (L/D 45) designed to be connected together (~500 g)
• Two DSM vertical mini-extruders (~15 g)
• Two Thermo-Haake MiniLab mini-extruders (~6 g)
• Thermo-Haake mini injection machine
• Injection machine Ray Ran
• babyplast micro moulding machine from MARTIPLAST
• NETSTAL injection moulding machine
• Rondol two-roll mill (roll diam.: 80 mm)
• 4 Brabender internal mixers (~ 50 g polymer)
• Brabender single screw extruder (19 mm, 25D) equipped with a ribbon die (50 x 0.5 mm) and a conveyor belt or a double-string die
• Thermo-Haake pelletizer
• MACGI single screw extruder (14 mm, 24D) equipped with different dies. Designed for raw material testing (hundred of grams to some kg/h) and R&D works, it can be also used as co-extruder (working positions - horizontal, vertical, angles)
• Agila PE20 hydraulic press (high and low temperatures)
• Carver manual press (25x25 cm² plates)
• Ray Ran cutting machine
• Hess 5 MP hydraulic press for ASTM norms-based samples cutting
• Ray-Ran CNC milling machine for sample shaping
• Rondol mini-mixer (0-4000 rpm)
• Plastograph internal mixer (Brabender, 40-60 cm³, up to 200 N.m)
• Vertical twin-screw microcompounder (XPlore, 15 cm³, up to 10 000 N)
• Micro fibre and cast film lines (XPlore)
• MiniLab horizontal twin-screw microcompounder (Thermo Haake, 7 cm³)
• Manual hydraulic press (Carver, up to 10 bars)Micro injection moulder (Xplore, 5-10 cm³)

• UV/visible thermostated spectrophotometer Varian Cary 50 equipped with an external optical fiber
• (2 multinuclear NMR 500 et 300 MHz available in the department)
• Fourier Transform Infra-Red Bruker Tensor 27 Spectrometer (6000 – 600 cm^-1) equipped with a Miracle micro-ATR from Pike
• Fourier Transform Infra-Red Biorad Excalibur Spectrometer (4000 – 700 cm-1) equipped with a Split-pea micro-ATR from SAFIR
• Programmable Brookfield DV-II viscosimeter
• Temperature-controlled tensiometer (DSA10-MK2 from Krüss) for static and dynamic measure of surface tension by the pendant drop and the contact angle methods

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• High resolution thermogravimetric analyser (TA Instrument TGA Q5000) equipped with an autosampler and simultaneously coupled to a Balzers Thermostar quadrupolar mass spectrometer and a Fourier Transform Infra-Red Bruker Tensor 27 spectrometer equipped with a gas cell at 230°C and HS MCT detector : TGA-FTIR/MS
• High resolution thermogravimetric analyser (TA instrument Hi-Res TGA 2950) simultaneously coupled to a Fourier Transform Infra-Red Biorad Excalibur spectrometer: TGA-FTIR
• Two standard thermogravimetric analysers from TA Instrument (TGA Q500 and Q50)
• Temperature modulated Differential Scanning Calorimeter from TA Instrument (DSC Q2000) equipped with an autosampler (-160 to + 750°C)
• Temperature modulated Differential Scanning Calorimeter from TA Instrument (MDSC 2920)
• Two differential scanning calorimeters from TA Instrument (Q200) equipped with the T-zero calorimetric system reducing the signal to noise ratio
• Two dynamic Mechanical Thermal Analysers from TA Instrument (DMA Q800 and 2980) equipped for three-point bending, tensile, compression, single and dual cantilever analyses
• Calcination Nabertherm 3 L oven (T < 1100°C)
• Rheometer MCR 302 (Anton Paar) with accessories for UV, dielectrical and electrical measurements
• Lab Process mixer for functionnalisation of powders (Zeppelin)
• Dynamic Mechanical Thermal Analyzer (TA Instrument- Q800, equipped with three-point bending, tensile, compression, single and dual cantilever and a humidity chamber)

• Automatic Karl-Fisher MKC500 titration
• Automatic pH M 210 Radiometer

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• Universal tensile testing machine (ZwickRoell, equipped with tensile, 3-points bending, compression clamps and humidity chamber for gels).